EXP_NMR: expnmr_00324


Sample:

NAME: Cyclohexylamine VENDOR: Aldrich
CAT_ID: 240648 CAS: 108-91-8

Condition:

TEMPERATURE: 298 K SAMPLE_CONCEN: 100 mM
SOLVENT: D2O BUFFER: 50mM Sodium Phosphate
BUFFER2: 500uM NaAzide REFERENCE: 500uM DSS
pH: 7.4 NMR INSTRUMENT: BRUKER DMX 500

Experiments:

1. 1D-1H: Peaks_list
1D 1H1D 1H ZOOM
2. 2D-[1H,1H]-TOCSY: Peaks_list
2D 1H-TOCSY 2D TOCSY ZOOM

Contour Level increase

Contour Level decrease

3. 1D-13C: Peaks_list
1D 13C1D 13C ZOOM
4. 1D-13C DEPT90: Peaks_list
1D 13C DEPT901D 13C DEPT90 ZOOM
5. 1D-13C DEPT135: Peaks_list
1D 13C DEPT1351D 13C DEPT135 ZOOM
6. 2D-[1H,13C]-HSQC: Peaks_list
2D [1H,13C]-HSQC 2D HSQC ZOOM

Contour Level increase

Contour Level decrease

7. 2D-[1H,13C]-HMBC: Peaks_list
2D [1H,13C]-HMBC 2D HMBC ZOOM

Contour Level increase

Contour Level decrease


Assignments:

Please find the chemical shift assignments, if available, in corresponding MMCD standard compound detail record page

Data collected and processed by Qiu Cui, Please contact MMCD if any question

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