EXP_NMR: expnmr_00455


Sample:

NAME: 2-Hydroxyisocaproic acid VENDOR: sigma
CAT_ID: CAS:

Condition:

TEMPERATURE: 298 K SAMPLE_CONCEN: 100 mM
SOLVENT: D2O BUFFER: 50mM Sodium Phosphate
BUFFER2: 500uM NaAzide REFERENCE: 500uM DSS
pH: 7.4 NMR INSTRUMENT: BRUKER DMX 500

Experiments:

1. 1D-1H: Peaks_list
1D 1H1D 1H ZOOM
2. 2D-[1H,1H]-TOCSY: Peaks_list
2D 1H-TOCSY 2D TOCSY ZOOM

Contour Level increase

Contour Level decrease

3. 1D-13C: Peaks_list
1D 13C1D 13C ZOOM
4. 1D-13C DEPT90: Peaks_list
1D 13C DEPT901D 13C DEPT90 ZOOM
5. 1D-13C DEPT135: Peaks_list
1D 13C DEPT1351D 13C DEPT135 ZOOM
6. 2D-[1H,13C]-HSQC: Peaks_list
2D [1H,13C]-HSQC 2D HSQC ZOOM

Contour Level increase

Contour Level decrease

7. 2D-[1H,13C]-HMBC: Peaks_list
2D [1H,13C]-HMBC 2D HMBC ZOOM

Contour Level increase

Contour Level decrease


Assignments:

Please find the chemical shift assignments, if available, in corresponding MMCD standard compound detail record page

Data collected and processed by Qiu Cui, Please contact MMCD if any question

About Us | Site Map | NMRFAM Policy | Contact Us | ©2007 MMCD